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Beilstein J. Org. Chem. 2012, 8, 890–896, doi:10.3762/bjoc.8.101
Graphical Abstract
Figure 1: Structures of azobenzene thioesters, Nα-ligation auxiliaries and peptides for the application in li...
Scheme 1: Structural differences between the trans- and the cis-state of azopeptides with a SKV PDZ binding m...
Figure 2: Structure of the glycine-linked auxiliary conjugates 7 and 8.
Scheme 2: Solid-phase synthesis of the ligation-mediating peptides 3–5.
Scheme 3: Reduction of the diazene unit of 4,4'-AMPB thioesters and peptides during aliphatic thiol-based Nα-...
Scheme 4: Synthesis of the azopeptides 16/17 by final TFA cleavage of the Boc-protecting groups, and of the a...
Beilstein J. Org. Chem. 2009, 5, No. 25, doi:10.3762/bjoc.5.25
Scheme 1: Photochromism of 2H-chromenes.
Scheme 2: Synthesis of functionalized pyrans from 2-bromo-3H-naphtho[2,1-b]pyrans and 3-bromo-2H-1-benzopyran...
Scheme 3: Synthesis of the 2-bromo-3H-naphtho[2,1-b]pyran 1 and the 3-bromo-2H-1-benzopyrans 2a/b.
Scheme 4: Ring contraction observed during the cyanation approach towards the synthesis of 3.
Scheme 5: Palladium-catalyzed Sonogashira-coupling of 2-bromo-3H-naphtho[2,1-b]pyran 1.
Scheme 6: Palladium-catalyzed cyanation and carbonylation of 3-bromo-2H-1-benzopyrans 2a/b.
Figure 1: Data from time-resolved measurements of compound 5a. a) and b): Results from fs-pump-probe-spectros...